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Adenosine 5'-monophosphate monohydrate Basic information Product Name: Adenosine 5'-monophosphate monohydrate Synonyms: ADENOSINE 5'-MONOPHOSPHATE FREE ACID97+% FROM YEAS;5'-AMP=Adenylicacid;ADENOSINE-5'-MONOPHOSPHATE 1-HYDRATE;5'-AMP H2O;5'-AMP MONOHYDRATE;ADENOSINE 5'-MONOPHOSPHATE MONOHYDRATE;ADENOSINE 5'-MONOPHOSPHORIC ACID MONOHYDRATE;ADENYLIC ACID MONOHYDRATE CAS: 18422-05-4 MF: C10H16N5O8P MW: 365.24 EINECS: 200-500-0 Product Categories: nucleoside;Nucleotides and Nucleic Acids Mol File: 18422-05-4.mol   Adenosine 5'-monophosphate monohydrate Chemical Properties Melting point 183-188 °C (dec.)(lit.) alpha -48 º (c=2% in 2% NaOH) FEMA 4224 | ADENOSINE MONOPHOSPHATE; MONOSODIUM, OR DISODIUM ADENYLATE storage temp. 2-8°C solubility H2O: with addition of mild alkalisoluble Merck 14,158 BRN 5205540 CAS DataBase Reference 18422-05-4(CAS DataBase Reference)   Safety Information Hazard Codes Xi Risk Statements 36/37/38 Safety Statements 26-36 WGK Germany 3 RTECS AU7480500 F 8-10-21 TSCA Yes MSDS Information Provider Language SigmaAldrich English ALFA English   Adenosine 5'-monophosphate monohydrate Usage And Synthesis Chemical Properties White crystalline powder Uses Nutrient;Ca++ channel block Purification Methods The acid has been recrystallised from H2O (fine needles) and is freely soluble in boiling H2O. It crystallises also from H2O on addition of acetone. Alternatively purify it by chromatography on Dowex 1 (in formate form), eluting with 0.25M formic acid. It is then adsorbed onto charcoal (which had been boiled for 15minutes with M HCl, washed free of chloride and dried at 100o) and recovered by stirring three times with isoamyl alcohol/H2O (1:9 v/v). The aqueous layer from the combined extracts is evaporated to dryness under reduced pressure, and the product is crystallised twice from hot H2O. [Morrison & Doherty Biochem J 79 433 1961]. It has max 259nm ( 15,400) in H2O at pH 7.0. [Alberty et al. J Biol Chem 193 425 1951, Martell & Schwarzenbach Helv Chim Acta 39 653 1956]. The acridinium salt has m 208o [Baddiley & Todd J Chem Soc 648 1947, Pettit Synthetic Nucleotides, van Nostrand-Reinhold, NY, Vol 1 252 1972, NMR: Sarma et al. J Am Chem Soc 96 7337 1974, Norton et al. J Am Chem Soc 98 1007 1976, IR of diNa salt: Miles Biochem Biophys Acta 27 324 1958]. [Beilstein 26 III/IV 3615.]   Adenosine 5'-monophosphate monohydrate Preparation Products And Raw materials